Laboratory of instrumental analysis
executive & GC operator: Robert Vícha, 576 031 103
technician & DI and EA operator: Lenka Trhlíková, 576 031 003
ion trap operator: Michal Rouchal, 576 031 433
itc operator: Petra Branná, 576 031 003
- Analysis form
- Operating rules
FACILITIES
- Ion trap BRUKER amaZon X with LC DIONEX ultimate 3000
- VP-ITC
- Headspace utility for GC - MS
- GC - MS
Reference for your papers:
GC–MS analyses were run on a Shimadzu QP–2010 instrument with integrated MS library NIST 02.
Option GC:
Supelco SLB–5ms (30 m, 0.25 mm) column and He as carrier gas at constant linear velocity
(38 cm•s–1) were used; GC method: 100 °C/7 min, 25 °C/min to 250 °C, hold for required time, IS 200 °C/70 eV.
Option DI:
Samples were prepared by drying of 10ul of solution (0.03 mg/ml) in dichloromethane in DI cuvette at 50°C.
DI method: 80°C/1 min, 40°C/min to 350°C, hold for required time, IS 200 °C/70 eV.
Only m/z signals exceeding relative abundance of 5% are listed.
- GC - FID
- Elemental analysis
Reference for your papers:
Elemental analyses (C, H, N, S) were run on Thermo Fisher Scientific Flash EA 1112.
Note: Variables are accentuated with italics.