Laboratory of instrumental analysis

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executive & GC operator: Robert Vícha, 576 031 103
technician & DI and EA operator: Lenka Trhlíková, 576 031 003
ion trap operator: Michal Rouchal, 576 031 433
itc operator: Petra Branná, 576 031 003

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• Analysis form
• Operating rules


FACILITIES


• Ion trap BRUKER amaZon X with LC DIONEX ultimate 3000
• VP-ITC
• Headspace utility for GC - MS
• GC - MS
  Reference for your papers:
  GC–MS analyses were run on a Shimadzu QP–2010 instrument with integrated MS library NIST 02.
  
  Option GC:
  Supelco SLB–5ms (30 m, 0.25 mm) column and He as carrier gas at constant linear velocity (38 cm•s^–1) were used; GC method: 100 °C/7 min, 25 °C/min to 250 °C, hold for required time, IS 200 °C/70 eV.
  
  Option DI:
  Samples were prepared by drying of 10ul of solution (0.03 mg/ml) in dichloromethane in DI cuvette at 50°C.
  DI method: 80°C/1 min, 40°C/min to 350°C, hold for required time, IS 200 °C/70 eV.
  
  Only m/z signals exceeding relative abundance of 5% are listed.



• GC - FID
• Elemental analysis
  
  Reference for your papers:
  Elemental analyses (C, H, N, S) were run on Thermo Fisher Scientific Flash EA 1112.




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Note: Variables are accentuated with italics.